Research & Scientific Output

Laboratory Research & Publications

From synthesizing novel anisotropic single crystals to designing cryogenic optical trains, probing nanoscale polaritonic light-matter interactions, and publishing experimental findings at national laboratories.

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Appointments & Labs

Laboratory Research

5 Appointments

Purdue University · West Lafayette, IN

Nanometa Group - Purdue Birck Nanotechnology Center

Oct 2025 - Present

Student Researcher (PIs: V.M. Shalaev, A. Boltasseva, A. Banerjee)

Oct 2025 - Present

Synthesized high-purity single crystals of anisotropic 2D MoOCl2 oxyhalides via Chemical Vapor Transport (CVT), confirming monoclinic C2/m phase purity via Single-Crystal XRD (R-factor = 3.21%) and Raman spectroscopy. Mapped propagation of visible-frequency Hyperbolic Plasmon Polaritons (HPPs) in MoOCl2 using s-SNOM near-field optical microscopy under 1.8 µm excitation, demonstrating extreme spatial mode compression down to 483 nm (n = 1) key to next-generation sub-diffraction nanophotonic computing, sensing, and superlensing.

  • CVT growth of high-purity anisotropic MoOCl2 single crystals
  • Single-Crystal XRD confirmation (R-factor = 3.21%, monoclinic C2/m)
  • s-SNOM near-field optical microscopy mapping hyperbolic polaritons with mode compression to 483 nm

Open Quantum Initiative (OQI) & Purdue SURF Fellow (PI: Vladimir Shalaev)

May 2026 - Jul 2026

Selected for the Open Quantum Initiative (OQI) Fellowship by Chicago Quantum Exchange (CQE) and Purdue SURF Fellowship to execute advanced quantum nanophotonics research; awarded SURF honors. Achieved up to 350% polarization-dependent single photon emission modulation at 4.5 K by engineering hBN/WSe2/MoOCl2 2D heterostructures with ALD Al2O3 dielectric spacers, laying groundwork for tunable quantum photonic components. Engineered the first deterministically twisted MXene bilayers via AFM lithography and polymer dry-transfer techniques to explore moiré-induced optoelectronic phenomena. Constructed custom Near-Infrared (NIR) cryogenic optical collection and excitation setups with high-NA objectives and spectral filters for low-temperature exciton and silicon nitride single photon emission diagnostics.

  • Awarded prestigious regional OQI Fellowship & Purdue SURF Honors
  • Achieved up to 350% polarization-dependent single photon emission modulation at 4.5 K
  • Deterministic AFM dry-transfer twisting of MXene and TMD heterostructures
  • Constructed custom NIR cryogenic optical collection setups (4.5 K) with high-NA optics

Core contributions

·Demonstrated extreme spatial mode compression (483 nm) of visible hyperbolic polaritons in 2D MoOCl2 crystals.

·Engineered hBN/WSe2/MoOCl2 van der Waals heterostructures achieving 350% single photon emission modulation at 4.5 K.

·Built custom cryogenic optical excitation/collection setups with sub-micron spatial resolution.

Oak Ridge National Laboratory (ORNL) · Oak Ridge, TN

Quantum Heterostructures Group - Oak Ridge National Laboratory

RSI Research Intern (PI: Benjamin Lawrie)

May 2025 - Aug 2025

Designed and assembled a custom room-temperature quantum sensing microscope system integrated with a compact optics train. Developed a novel quantum sensing fabrication protocol for shallow boron vacancy (V_B^-) spin defects in hexagonal boron nitride (hBN). Quantified quantum decoherence from gold waveguides by automating nanoscale Johnson noise measurements in Python and MATLAB, focusing on T1 relaxometry and distance dependence to address key limits in quantum device scaling. Patterned gradient defect dosage arrays via Helium Ion Microscope (HIM) irradiation to map spin-spin interactions.

Core contributions

·Engineered a room-temperature quantum sensing microscope from scratch with custom optical train.

·Established fabrication protocol for shallow V_B^- spin defects in hexagonal boron nitride (hBN).

·Automated T1 relaxometry nanoscale Johnson noise measurements to probe quantum decoherence mechanisms.

Purdue University · West Lafayette, IN

Quantum Matter and Devices Group - Purdue University

Student Researcher (PI: Yong P. Chen)

Jan 2025 - Jun 2025

Fabricated twisted TMD semiconductor heterostructures exploiting inter-layer superlubricity for precise twist-angle control, engineering tunable moiré superlattices for reconfigurable quantum electronics.

Core contributions

·Investigated dynamic bilayer twisting utilizing structural superlubricity.

·Explored tunable moiré superlattices in transition metal dichalcogenide (TMD) bilayers.

·Authored technical report on dynamic twist-angle manipulation under electric and magnetic fields.

University of Tennessee, Knoxville · Knoxville, TN

Emergent Crystalline Matter Group - University of Tennessee, Knoxville

Full-Time Paid Research Intern (PI: David Mandrus)

Jul 2023 - Aug 2024

Grew 15+ novel single crystals (high-entropy alloys, Kagome lattices, topological superconductors) via flux and CVT growth methods, validating phase purity via XRD, SQUID, and PPMS. Accelerated crystal synthesis by creating CrysTool Hub, an open-source web application (Next.js, Python, Flask) that automates stoichiometric calculations and furnace plans. Still used to this day.

Core contributions

·Synthesized 15+ novel single crystals (Kagome lattices, topological superconductors, HEAs).

·Characterized phase purity and magnetic properties using Powder XRD, SQUID magnetometry, and PPMS.

·Developed CrysTool Hub to automate multi-component stoichiometry and temperature ramps for synthesis.

Los Alamos National Laboratory / DOE / DTRA · Albuquerque, NM

Joint Science & Technology Institute (JSTI) West

Green Microbial Factory Group Member (PI: Raul Gonzalez)

Jun 2022

Awarded a fully-paid internship by the DOE & DTRA to work with Los Alamos National Lab scientists. Studied and presented on the biotechnological potential of cyanobacteria, finding optimum strains for photosynthetic bioplastic production.

Core contributions

·Selected for competitive DOE/DTRA defense science research institute.

·Analyzed flow cytometry data of cyanobacteria strains for photosynthetic bioplastic synthesis.

Research Output

Publications & Talks

3 Selected Works

Technical papers, invited oral presentations, and symposium contributions covering anisotropic 2D crystals, optical defect magnetometry, and superlubricity.

July 2026
Technical Paper

Orientation-Dependent Excitonic Coupling and Purcell Enhancement in MoOCl2-TMDC Heterostructures

Manley, R. Y., Banerjee, A., Shalaev, V. M., Boltasseva, A., et al.

Purdue SURF Honors Technical Paper & Technical Poster Presentation

Venue Link ↗
March 2026
Invited Oral Presentation

Probing Johnson Noise with Shallow Spin Defects in 2D hBN

Manley, R. Y., Lawrie, B., et al.

Symposium Oral Presentation, TMS Annual Meeting & Exhibition, San Diego, CA

Venue Link ↗
May 2025
Technical Report

Dynamic Bilayer Twisting with Superlubricity in 2D Semiconductors

Manley, R. Y.

Purdue School of Electrical and Computer Engineering Technical Report

Venue Link ↗PDF ↗

Core Competencies

Technical Skills

4 Domains

Nanofabrication & Crystal Growth

Chemical Vapor Transport (CVT) Growth · Flux Single Crystal Synthesis · 2D Micromechanical Exfoliation & Dry Stacking · AFM Nanolithography & Polymer Transfer · Helium Ion Microscope (HIM) Defect Patterning · Cleanroom Photolithography & ALD Spacers

Characterization & Cryogenics

s-SNOM Near-Field Optical Microscopy · Single-Crystal & Powder XRD · Confocal Raman & Photoluminescence (PL) · ODMR & T1 Spin Relaxometry · Liquid Helium Cryogenics (4.5 K) · SQUID Magnetometry & PPMS Transport

Programming & Computation

Python (Qiskit, NumPy, SciPy, TensorFlow) · TypeScript, JavaScript, React, Next.js · C, C++, SystemVerilog, Java · MATLAB, R, LaTeX · Quantum ESPRESSO (DFT) & SRIM Ion Stopping · Git, Linux, Node.js, Flask

Hardware, Circuits & CAD

KiCad & Eagle PCB Design · LTspice Circuit Simulation · Onshape & Autodesk Fusion 360 · Arduino & STM32 Microcontroller Firmware · High-NA Optical Train Assembly & Alignment · Motorized Precision Gimbal Actuation